
Titanium dioxide and Titanium dioxide loaded groundnut shell activated carbon photocatalytic activity were synthesized by sol-gel technique. The preparation of TiO2 and TiO2/GNSAC photocatalysts were achieved by titanium tetra isopropoxide and 2-propanol as common starting materials and annealed the product at 500 °C for 2 h to get anatase phase, respectively. The prepared materials were characterized by X-ray diffraction analysis (XRD), Fourier transform infrared spectroscopy (FT-IR), and UV-Vis-diffuse reflectance spectroscopy (DRS), The photocatalytic activity was tested and compared with that of TiO2 and TiO2/GNSAC on the degradation of methylene blue (MB) and brilliant green (BG) in an aqueous solutions using sunlight radiation. The adsorption kinetics followed both the pseudo-first-order and second-order giving a better fit. The TiO2/GNSAC removal over 95.39% of BG and 81.57% of MB dyes and its adsorption was fitted best to all models.